I'm not familiar with that puzzle, but if that's true it's got to be a prime candidate.
I'm going to nominate "Infection" - the Go-style bacteria puzzle in The 7th Guest. Not only was there NO "solution" - you just had to improve at the game until you got very lucky and outplayed the devious (and ingenious) AI - but, for me at least, it came early in the game and really killed momentum.
If Stauf had simply put in a dozen variants of the bacteria puzzle in his mansion, no one would ever have learned his secrets, trust me. He would've been home free.
A lot of people nominate the "retrieve the key" sequence in The Longest Journey, but I didn't have problems with that, and my wife literally solved it at first glance.
Looking back, I thought that the entire first sequence of KQIII was devilishly hard, ESPECIALLY the spell-making.
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